Design and Characterization of a Microwave Transducer for Gas Sensing Applications

Gas sensors have wide applications in several fields, spanning diverse areas such as environmental monitoring, healthcare, defense, and the evaluation of personal and occupational exposure to hazardous chemicals. Different typologies of gas sensors have been proposed over the years, such as optical, electrochemical, and metal oxide gas sensors. In this paper, a relatively new typology of gas sensors is explored: the microwave gas sensor. It consists of a combination of a microwave transducer with a nanostructured sensing material deposited on an interdigitated capacitor (IDC). The device is designed and fabricated on a Rogers substrate (RO4003C) using microstrip technology, and investigated as a microwave transducer over the frequency range from 1 GHz to 6 GHz by measuring the scattering (S) parameters in response to gas adsorption and desorption. The sensing material is based on a nano-powder of barium titanate oxalate with a coating of urea (BaTiO(C2 O4)2 /CO(NH2)2). It is deposited on the IDC surface by drop coating, thus creating a sensing film. The developed prototype has been tested toward different oxygen (O2) concentrations and exhibits a sensitivity of 28 kHz/%O2. Special attention has been devoted to the measurement process. Besides the canonical short-open-load-thru (SOLT) calibration of the measured S-parameters, a thru-reflect-line (TRL) calibration has been performed in order to get rid of the parasitic electromagnetic (EM) contributions of the board connectors and the feedlines, thus moving the measurement reference planes to the edges of the IDC.