Essential oils from the aerial parts of Sicilian Teucrium flavum L., isolated by using microwave-assisted hydrodistillation (MHD), were analyzed for the first time at various seasonal stages (vegetative and budding stage) by means of GC/MS and GC-FID; the flowers and fruits were also subjected to examination. More than 80 compounds were identified as oil components. The leaf, flower and fruit oils were characterized by a predominance of sesquiterpenes, such as beta-caryophyllene (3-5 g/100 g), germacrene D (4-14 g/100 g), beta-bisabolene (32-49 g/100 g); the total amount of sesquiterpene hydrocarbons contained in each oil was 56-70 g/100 g, the oxygenated derivatives were in the range of 9-20 g/100 g. The monoterpene hydrocarbons in all samples (leaves, flowers, fruits) were contained in very low amounts, from 0.2 to 1.6 g/100 g, and were the least representative fraction of the oils. Oxygenated aliphatic compounds, especially esters, were also detected. The results can be useful to support, by means of a safe reliable sample preparation (MHD) and analytical (GC) technique, the research on medicinal plants belonging to Mediterranean flora.
Seasonal Variations of Teucrium flavum L. Essential Oil
COSTA, ROSARIA;DUGO, Giovanni;MONDELLO, Luigi;
2010-01-01
Abstract
Essential oils from the aerial parts of Sicilian Teucrium flavum L., isolated by using microwave-assisted hydrodistillation (MHD), were analyzed for the first time at various seasonal stages (vegetative and budding stage) by means of GC/MS and GC-FID; the flowers and fruits were also subjected to examination. More than 80 compounds were identified as oil components. The leaf, flower and fruit oils were characterized by a predominance of sesquiterpenes, such as beta-caryophyllene (3-5 g/100 g), germacrene D (4-14 g/100 g), beta-bisabolene (32-49 g/100 g); the total amount of sesquiterpene hydrocarbons contained in each oil was 56-70 g/100 g, the oxygenated derivatives were in the range of 9-20 g/100 g. The monoterpene hydrocarbons in all samples (leaves, flowers, fruits) were contained in very low amounts, from 0.2 to 1.6 g/100 g, and were the least representative fraction of the oils. Oxygenated aliphatic compounds, especially esters, were also detected. The results can be useful to support, by means of a safe reliable sample preparation (MHD) and analytical (GC) technique, the research on medicinal plants belonging to Mediterranean flora.Pubblicazioni consigliate
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